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Back ChemicalBook Home>CAS DataBase List>13104-56-8More Spectrum> 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE(13104-56-8) 1H NMR

13104-56-8

4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE(13104-56-8) 1H NMR

Molecular FormulaC22H17N3O

Molecular Weight339.39

InChIInChI=1S/C22H17N3O/c1-26-18-10-8-16(9-11-18)17-14-21(19-6-2-4-12-23-19)25-22(15-17)20-7-3-5-13-24-20/h2-15H,1H3

InChIKey QAEWAYWLMREGRA-UHFFFAOYSA-N

SmilesC1(C2=NC(C3=NC=CC=C3)=CC(C3=CC=C(OC)C=C3)=C2)=NC=CC=C1

  • 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE(13104-56-8) <sup>1</sup>H NMR
    Mass

    MS-NW-6975          
    4-(p-methoxyphenyl)-2,6-di(2-pyridyl)pyridine
    C22H17N3O           (Mass of molecular ion:    339)
    

       Source Temperature: 200 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          18.0       1.5
          51.0       2.8
          52.0       1.0
          63.0       1.2
          78.0       5.2
          79.0       1.2
          89.0       1.1
          95.5       1.1
         134.0       1.4
         134.5       1.0
         135.0       1.3
         140.0       1.0
         147.0       1.6
         147.5       2.7
         148.0       5.1
         148.5       1.4
         153.5       1.5
         162.0       1.6
         164.0       1.0
         169.5       6.0
         170.0       1.7
         190.0       1.7
         191.0       3.2
         192.0       1.6
         216.0       1.4
         217.0       2.0
         218.0       4.1
         219.0       1.1
         234.0       2.2
         246.0       1.2
         261.0       7.3
         262.0       1.5
         267.0       1.0
         268.0       2.6
         269.0       1.4
         294.0       2.3
         295.0       5.6
         296.0       7.2
         297.0       2.2
         308.0       3.7
         309.0       2.1
         310.0       1.1
         311.0       2.7
         323.0       1.2
         324.0      14.3
         325.0       3.7
         338.0       7.6
         339.0     100.0
         340.0      24.9
         341.0       3.4
    

90 MHz in CDCl3

  • 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE(13104-56-8) <sup>1</sup>H NMR

    1H NMR 89.56 MHz
    C22 H17 N3 O 0.033 g : 0.5 ml CDCl3
    4-(p-methoxyphenyl)-2,6-di(2-pyridyl)pyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.66 B 8.66 C 8.60 D 7.82 E 7.81 F 7.27 G 6.973 J 3.809

         Hz     ppm     Int.
    

        779.50   8.704    135
        778.56   8.694    142
        777.63   8.683    158
        775.31   8.657    845
        767.75   8.573    148
        766.75   8.562    193
        765.75   8.551    125
        760.88   8.496     31
        707.25   7.897    104
        705.13   7.874    239
        702.88   7.849     84
        699.69   7.813    170
        697.81   7.792    190
        696.13   7.773    259
        693.06   7.739     62
        691.94   7.726    107
        690.00   7.705    102
        657.88   7.346    107
        656.50   7.331     99
        653.19   7.294     97
        651.81   7.278    112
        650.38   7.262     94
        649.13   7.248     85
        644.38   7.195     78
        631.44   7.051     37
        628.44   7.017    230
        626.25   6.993     69
        621.63   6.941     69
        619.50   6.918    179
        341.19   3.810   1000
    

in CDCl3

  • 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE(13104-56-8) <sup>1</sup>H NMR

KBr disc

  • 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE(13104-56-8) <sup>1</sup>H NMR

nujol mull

  • 4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE(13104-56-8) <sup>1</sup>H NMR

4'-(4-METHOXYPHENYL)-2,2':6',2''-TERPYRIDINE(13104-56-8) 1H NMR Atlas of Related Products

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