ChemicalBook >?? ???? >?? ??>?? ?? ???>Organic iron>5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE
5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE
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5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE ??
- ???
- 300 °C
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- Inert atmosphere,Room Temperature
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- ?? ??(λmax)
- 418 nm
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- ????. ?? ???, ??? ???? ????.
- InChIKey
- ZDYSAMCSFRQDMN-XBZZRTMISA-M
- CAS ??????
- 16456-81-8
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- ?? ? ???? ?? (GHS)
| ????? | 22-24/25 | ||
|---|---|---|---|
| WGK ?? | 3 | ||
| HS ?? | 29349990 |
5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE C??? ??, ??, ??
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dark red or purple powder??
Iron(III) meso-tetraphenylporphine chloride is used catalyzing reagent for silylation reactions.Purification Methods
Purify it by extraction from a thimble (Soxhlet) with CHCl3. Concentrate the extract to ca 10mL and add ca 80mL of hot MeOH. Dark blue crystals separate on cooling. It can be recrystallised several times from CHCl3/MeOH. Avoid prolonged heating. It is quite soluble in organic solvents but insoluble in pet ether. [Rothemund & Manotti J Am Chem Soc 70 1808 1948, UV: Dorough et al. J Am Chem Soc 73 4315 1951, Beilstein 26 III 1960.]5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE ?? ?? ? ???
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5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE ?? ??
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5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE ?? ??:
????? IX
ZINC MESO-TETRAPHENYLPORPHINE
5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE
FETPPS
5,10,15,20-TETRAKIS(PENTAFLUOROPHENYL)-21H,23H-PORPHINE IRON(III) CHLORIDE
5,10,15,20-TETRAKIS-(4-CARBOXYPHENYL)-PORPHYRIN-FE-(III) CHLORIDE
TPP
5,10,15,20-TETRAPHENYL-21H,23H-PORPHINE IRON(III) CHLORIDE
5,10,15,20-TETRAKIS(4-METHOXYPHENYL)-21H,23H-PORPHINE IRON(III) CHLORIDE
meso-Tetratolylporphyrin-Fe(III)chloride
5-(4-AMINOPHENYL)-10,15,20-TRIPHENYL-PORPHYRIN-FE(III) CHLORIDE
5-(4-HYDROXYMETHYLPHENYL)-10,15,20-TRIPHENYL-PORPHYRIN-FE(III) CHLORIDE
5-(4-HYDROXYPHENYL)-10,15,20-TRIPHENYL-PORPHYRIN-FE(III) CHLORIDE
5,10,15,20-TETRAKIS-(3-METHOXY-4-HYDROXY-PHENYL)-PORPHYRIN-FE(III) CHLORIDE
RARECHEM AS SA 0018
5,10,15,20-TETRAKIS-(4-AMINOPHENYL)-PORPHYRIN-FE(III) CHLORIDE
5-(4-CARBOXYPHENYL)-10,15,20-TRIPHENYL-PORPHYRIN-FE(III) CHLORIDE
5-(3-HYDROXYPHENYL)-10,15,20-TRIPHENYL-PORPHYRIN-FE(III) CHLORIDE