(S)-1-(4-Nitrophenyl)ethylamine hydrochloride
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- CAS-Nr.
- 57233-86-0
- Englisch Name:
- (S)-1-(4-Nitrophenyl)ethylamine hydrochloride
- Synonyma:
- (+)-Nitresolve;(R)-A-METHYL-4-NITROBENZYLAMINE HCL;BenzeneMethanaMine, a-Methyl-4-nitro-;METHYL-4-NITROBENZYLAMINEHYDROCHLORIDE;(R)-(-)-1-(4-NITROPHENYL)-ETHYLAMINE HCL;1-(4-nitrophenyl)ethylamine hydrochloride;(R)-(-)-ALPHA-METHYL-4-NITROBENZYLAMINE HCL;(R)-4-NITROPHENYL-1-ETHYLAMINE HYDROCHLORIDE;(R)-4-Nitro-α-methylbenzylamine hydrochloride;(r)-α-methyl-4-nitrobenzylamine hydrochloride
- CBNumber:
- CB6465238
- Summenformel:
- C8H11ClN2O2
- Molgewicht:
- 202.64
- MOL-Datei:
- 57233-86-0.mol
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(S)-1-(4-Nitrophenyl)ethylamine hydrochloride Eigenschaften
- Schmelzpunkt:
- 248-250 °C(lit.)
- alpha
- -6.5 º (c=1, 0.05N NaOH)
- storage temp.
- Inert atmosphere,Room Temperature
- Optische Aktivit?t
- [α]25/D +6.0°, c = 1 in 0.05 M NaOH
- BRN
- 3701567
- CAS Datenbank
- 57233-86-0(CAS DataBase Reference)
(S)-1-(4-Nitrophenyl)ethylamine hydrochloride Chemische Eigenschaften,Einsatz,Produktion Methoden
R-S?tze Betriebsanweisung:
R36/37/38:Reizt die Augen, die Atmungsorgane und die Haut.
S-S?tze Betriebsanweisung:
S26:Bei Berührung mit den Augen sofort gründlich mit Wasser abspülen und Arzt konsultieren.
S37/39:Bei der Arbeit geeignete Schutzhandschuhe und Schutzbrille/Gesichtsschutz tragen.
l?uterung methode
To ensure dryness, the hydrochloride (ca 175 g) is extracted with EtOH (3x100mL) and evaporated to dryness (any residual H2O increases the solubility in EtOH and lowers the yield). The hydrochloride residue is triturated with absolute EtOH and dried in vacuo. The product is further purified by refluxing with absolute EtOH (200 mL for 83g) for 1hour, and cool to 10o to give 76.6g of hydrochloride m 243-245o(dec). The free base is prepared by dissolving in N NaOH, extracting with CH2Cl2 (3 x 500mL), drying (Na2CO3), filtering, evaporating and distilling it. It has m 27o, b 119-120o/0.5mm (105-107o/0.5mm, 157-159o/9mm, d 1.1764, n 1.5688, [] ±17.7o (neat) [Perry et al. Synthesis 492 1977,ORD: Nerdel & Liebig Justus Liebigs Ann Chem 621 142 1959]. [Beilstein 12 IV 2451.]
(S)-1-(4-Nitrophenyl)ethylamine hydrochloride Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte
(S)-1-(4-Nitrophenyl)ethylamine hydrochloride Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.
Global( 117)Lieferanten
57233-86-0()Verwandte Suche:
- METHYL-4-NITROBENZYLAMINEHYDROCHLORIDE
- (R)-4-Nitro-α-methylbenzylamine hydrochloride
- Benzenemethanamine, .alpha.-methyl-4-nitro-, monohydrochloride, (.alpha.R)-
- (r)-α-methyl-4-nitrobenzylamine hydrochloride
- (R)-A-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE,97%
- (R)-(-)-1-(4-NITROPHENYL)-ETHYLAMINE HCL
- (R)-1-(4-NITROPHENYL)ETHYLAMINE HYDROCHLORIDE
- (R)-4-NITROPHENYL-1-ETHYLAMINE HYDROCHLORIDE
- (R)-(-)-ALPHA-METHYL-4-NITROBENZYLAMINE HCL
- (R)-ALPHA-METHYL-4-NITROBENZYLAMINE HYDROCHLORIDE
- (R)-(+)-ALPHA-METHYL-4-NITROBENZYLAMMONIUM CHLORIDE
- (R)-A-METHYL-4-NITROBENZYLAMINE HCL
- (R)-(+)-A-METHYL 4-NITROBENZYLAMINE HYDROCHLORIDE
- (S)-1-(4-Nitrophenyl)ethylamine hydrochloride
- 1-(4-nitrophenyl)ethylamine hydrochloride
- (+)-Nitresolve
- (R)-1-(4-nitrophenyl)ethanamine hydrochloride
- BenzeneMethanaMine, a-Methyl-4-nitro-
- (R)-alpha-Methyl-4-nitrobenzylaMine hydrochloride 97%
- (R)-α-Methyl-4-nitrobenzylamine hydrochloride
- Benzenemethanamine, α-methyl-4-nitro-, hydrochloride (1:1), (αR)-
- (αR)-α-methyl-4-nitro-Benzenemethanamine hydrochloride (1:1)
- (alphaR)-alpha-Methyl-4-nitro-benzenemethanamine HCl
- 57233-86-0
- Chiral Resolving Reagents
- Chiral Resolution Reagents
- Asymmetric Synthesis
