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Florantyron

Florantyrone Struktur
519-95-9
CAS-Nr.
519-95-9
Bezeichnung:
Florantyron
Englisch Name:
Florantyrone
Synonyma:
Zanchol;florantyrone;γ-Oxo-8-fluoranthenebutyric acid;b-(8-Fluoranthoyl)propionic acid;g-Oxo-8-fluoranthenebutanoic acid;3-(4-PHENYLBENZOYL)PROPIONIC ACID;4-(4-BIPHENYLYL)-4-OXOBUTYRIC ACID;b-(8-Fluoranthyloyl)propionic acid;8-Fluoranthenebutanoic acid, γ-oxo-;g-Fluoranthen-8-yl-g-oxybutyric acid
CBNumber:
CB5239126
Summenformel:
C20H14O3
Molgewicht:
302.32
MOL-Datei:
519-95-9.mol

Florantyron Eigenschaften

Schmelzpunkt:
184-187 °C(lit.)
Siedepunkt:
574.2±33.0 °C(Predicted)
Dichte
1.367±0.06 g/cm3(Predicted)
CAS Datenbank
519-95-9(CAS DataBase Reference)

Sicherheit

Kennzeichnung gef?hrlicher T
R-S?tze: 25
S-S?tze: 28-45
RIDADR  UN 2811 6.1/PG 3
WGK Germany  3
RTECS-Nr. DV1761000
Giftige Stoffe Daten 519-95-9(Hazardous Substances Data)

Florantyron Chemische Eigenschaften,Einsatz,Produktion Methoden

R-S?tze Betriebsanweisung:

R25:Giftig beim Verschlucken.

S-S?tze Betriebsanweisung:

S28:Bei Berührung mit der Haut sofort abwaschen mit viel . . . (vom Hersteller anzugeben).
S45:Bei Unfall oder Unwohlsein sofort Arzt zuziehen (wenn m?glich, dieses Etikett vorzeigen).

Originator

Zanchol,Searle,US,1957

Manufacturing Process

50 g of fluoranthene and 26 g of succinic anhydride in 500 cc of nitrobenzene were treated at 0°C to 5°C with 75 g of anhydrous aluminum chloride. The temperature was held at 0°C for 4 hours and then allowed gradually to come to room temperature. The reaction mixture was allowed to stand for 16 hours. The reaction mixture was then worked up. In so doing, the reaction mixture was decomposed with dilute HCl, the nitrobenzene was removed by steam distillation and the residue after filtration was dissolved in hot sodium carbonate solution and filtered free of a small amount of nonacidic material. Precipitation from solution with HCl gave a light yellow product which crystallized from a 50-50 mixture of dioxane alcohol as fine platelets which melted at 192°C to 194°C and showed a neutral equivalent of 308 which corresponds closely to the theoretical value of 302 for β-fluoranthoylpropionic acid.
25 g of the crude acid was dissolved in 100 cc of water containing 13 g of sodium carbonate. On cooling a thick syrup was obtained. On dilution to 1 liter precipitation started and after standing 16 hours, the solid which separated was filtered (filtrate treated as below), suspended in water, acidified with HCl and filtered. Crystallization from alcohol gave a light yellow material melting at 199°C to 200°C and having a neutral equivalent of 303.
The filtrate mentioned above, upon acidification thereof with HCl gave a darker acid which melted over a wide range, but had a neutral equivalent which also corresponds to that of β-fluoranthoylpropionic acid.

Therapeutic Function

Hydrocholeretic

Florantyron Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


Florantyron Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

Global( 30)Lieferanten
Firmenname Telefon E-Mail Land Produktkatalog Edge Rate
Hubei Jusheng Technology Co.,Ltd.
18871490254
linda@hubeijusheng.com CHINA 28172 58
Shaanxi Dideu Medichem Co. Ltd
+86-29-87569266 15319487004
1015@dideu.com China 3942 58
Mainchem Co., Ltd. +86-0592-6210733
sale@mainchem.com China 32343 55
Nanjing Shizhou Biology Technology Co.,Ltd 13675144456
sean.lv@synzest.com China 10784 58
Shaanxi Dideu Medichem Co. Ltd 029-61856358 15229202216
1020@dideu.com China 10011 58

519-95-9(Florantyron)Verwandte Suche:


  • florantyrone
  • GAMMA-OXO-[1,1'-BIPHENYL]-4-BUTANOIC ACID
  • GAMMA-OXO(1,1'-BIPHENYL)-BUTANOIC ACID
  • 4-Fluoranthen-8-yl-4-oxobutanoic acid
  • b-(8-Fluoranthoyl)propionic acid
  • b-(8-Fluoranthyloyl)propionic acid
  • g-Fluoranthen-8-yl-g-oxybutyric acid
  • g-Oxo-8-fluoranthenebutanoic acid
  • Zanchol
  • γ-Oxo-8-fluoranthenebutyric acid
  • 4-(4-BIPHENYLYL)-4-OXOBUTYRIC ACID
  • 3-(4-PHENYLBENZOYL)PROPIONIC ACID
  • 4-(fluoranthen-8-yl)-4-oxobutyric acid
  • 8-Fluoranthenebutanoic acid, γ-oxo-
  • 519-95-9
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