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N-(PHENYLTHIO)PHTHALIMIDE

N-(PHENYLTHIO)PHTHALIMIDE Struktur
14204-27-4
CAS-Nr.
14204-27-4
Englisch Name:
N-(PHENYLTHIO)PHTHALIMIDE
Synonyma:
N-(PHENYLTHIO)PHTHALIMIDE;N-(Phenylthio)phthalimide>N-(Phenylthio)phthalimide;2-(Phenylthio)isoindoline-1,3-dione;2-(Phenylthio)-1,3-isoindolinedione;2-(Phenylthio)-1H-isoindol-1,3(2H)-dione;2-(Phenylthio)-1H-isoindole-1,3(2H)-dione;1H-Isoindole-1,3(2H)-dione, 2-(phenylthio)-
CBNumber:
CB1240906
Summenformel:
C14H9NO2S
Molgewicht:
255.29
MOL-Datei:
14204-27-4.mol

N-(PHENYLTHIO)PHTHALIMIDE Eigenschaften

Schmelzpunkt:
160-163 °C(lit.)
Siedepunkt:
432.2±28.0 °C(Predicted)
Dichte
1.42±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
L?slichkeit
DMSO: soluble25mg/mL, clear, yellow
pka
-3.05±0.20(Predicted)
Aggregatzustand
powder to crystal
Farbe
White to Light yellow
CAS Datenbank
14204-27-4
Sicherheit
  • Risiko- und Sicherheitserkl?rung
  • Gefahreninformationscode (GHS)
S-S?tze: 24/25
WGK Germany  3
HS Code  29309090
Bildanzeige (GHS) GHS hazard pictograms
Alarmwort Warnung
Gefahrenhinweise
Code Gefahrenhinweise Gefahrenklasse Abteilung Alarmwort Symbol P-Code
H302 Gesundheitssch?dlich bei Verschlucken. Akute Toxizit?t oral Kategorie 4 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P270, P301+P312, P330, P501
H315 Verursacht Hautreizungen. Hautreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P302+P352, P321,P332+P313, P362
H319 Verursacht schwere Augenreizung. Schwere Augenreizung Kategorie 2 Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" /> P264, P280, P305+P351+P338,P337+P313P
H335 Kann die Atemwege reizen. Spezifische Zielorgan-Toxizit?t (einmalige Exposition) Kategorie 3 (Atemwegsreizung) Warnung GHS hazard pictogramssrc="/GHS07.jpg" width="20" height="20" />
Sicherheit
P261 Einatmen von Staub vermeiden.
P305+P351+P338 BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach M?glichkeit entfernen. Weiter spülen.

N-(PHENYLTHIO)PHTHALIMIDE Chemische Eigenschaften,Einsatz,Produktion Methoden

synthetische

(a) Preparation of benzenesulfenyl chloride. To a stirred solution of 55 gm (0.5 mole) of benzene thiol in 300 ml of η -pentane at 0°C is added chlorine gas until an assay (GC) of the resulting red-orange solution shows quantitative conversion to the sulfenyl chloride. The reaction usually re­quires about 39 gm (0.6 mole) of chlorine.
(b) Reaction of benzenesulfenyl chloride with phthalimide. To a stirred solution of 73.5 gm (0.5 mole) of phthalimide in 200 ml of dimethylforma-mide is first added 60 gm (0.6 mole) of triethylamine. Then the sulfenyl chloride solution from (a) is slowly added dropwise. The reaction mixture is stirred for \ hr, poured into 2 liters of cold water, filtered, and dried to afford 121 gm (95%), m.p. 160-161°C (recrystallized from ethanol).
Complex imides such as camphorimide and 9,10-dihydroanthracene-9,10-endo-a,/3-succinimide have been alkylated in methylene dichloride with alkyl halides, using tetrabutylammonium bromide as a phase-transfer catalyst and aqueous potassium hydroxide as a base.
Preparation of N-(Phenylthio)phthalimide

N-(PHENYLTHIO)PHTHALIMIDE Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte

1H-Isoindol-1-one, 3-hydroxy- N-TERT-BUTYLBENZENESULFENAMIDE ETHYL 4-PHENYLSULFANYLBENZOATE

N-(PHENYLTHIO)PHTHALIMIDE Anbieter Lieferant Produzent Hersteller Vertrieb H?ndler.

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14204-27-4()Verwandte Suche:

  • N-(Phenylthio)phthalimide
  • 2-(Phenylthio)-1,3-isoindolinedione
  • 2-(Phenylthio)isoindoline-1,3-dione
  • N-(PHENYLTHIO)PHTHALIMIDE
  • N-(Phenylthio)phthalimide>
  • 1H-Isoindole-1,3(2H)-dione, 2-(phenylthio)-
  • 2-(Phenylthio)-1H-isoindole-1,3(2H)-dione
  • 2-(Phenylthio)-1H-isoindol-1,3(2H)-dione
  • 14204-27-4
  • Building Blocks
  • Others
  • Organic Building Blocks
  • Sulfur Compounds
  • Sulfur Compounds (for Synthesis)
  • N-Substituted Phthalimides
  • N-Substituted Maleimides, Succinimides & Phthalimides
  • N-Substituted Phthalimides
  • Sulfur Compounds (for Synthesis)
  • Synthetic Organic Chemistry
  • Organic Building Blocks
  • Others
  • Sulfur Compounds
  • Building Blocks
  • Chemical Synthesis
  • Organic Building Blocks
  • Sulfur Compounds
  • N-Substituted Maleimides, Succinimides & Phthalimides
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