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ChemicalBook--->CAS DataBase List--->634-66-2

634-66-2

634-66-2 Structure

634-66-2 Structure
IdentificationMore
[Name]

1,2,3,4-Tetrachlorobenzene
[CAS]

634-66-2
[Synonyms]

1,2,3,4-TETRACHLOROBENZENE
1,2,3,4-tcb
1,2,3,4-tetrachloro-benzen
tetrachlorobenzene(non-specificname)
Tetrachlorobenzene
1,2,3,4-TETRACHLOROBENZENE, 500MG, NEAT
1,2,3,4-TETRACHLOROBENZENE, 1X1ML MEOH 2 000UG/ML
1,2,3,4-TETRACHLOROBENZENE, TECH., 90%
1,2,3,4-TETRACHLOROBENZENE PESTANAL,100
1,2,3,4-tetrachlorobenzene solution
BENZENE,1,2,3,4-TETRACHLORO-
Tetrachlorobenzene, 1,2,3,4-
[EINECS(EC#)]

211-214-0
[Molecular Formula]

C6H2Cl4
[MDL Number]

MFCD00000538
[Molecular Weight]

215.89
[MOL File]

634-66-2.mol
Chemical PropertiesBack Directory
[Appearance]

WHITE CRYSTALLINE SOLID
[Melting point ]

44 °C
[Boiling point ]

254 °C761 mm Hg(lit.)
[density ]

1,73 g/cm3
[vapor pressure ]

1.5 (extrapolated from vapor pressures determined at higher temperatures, Tesconi andYalkowsky, 1998)
[refractive index ]

1.5348 (estimate)
[Fp ]

>230 °F
[storage temp. ]

APPROX 4°C
[solubility ]

0.0028g/l
[form ]

neat
[color ]

White crystals or needles
[Water Solubility ]

5.92mg/L(25 ºC)
[BRN ]

1910025
[Henry's Law Constant]

3.6 at 10 °C (Koelmans et al., 1999)
[Dielectric constant]

3.2000000000000002
[Uses]

Component of dielectric fluids, synthesis.
[CAS DataBase Reference]

634-66-2(CAS DataBase Reference)
[EPA Substance Registry System]

1,2,3,4-Tetrachlorobenzene (634-66-2)
Safety DataBack Directory
[Hazard Codes ]

Xn,T,F
[Risk Statements ]

R22:Harmful if swallowed.
R39/23/24/25:Toxic: danger of very serious irreversible effects through inhalation, in contact with skin and if swallowed .
R23/24/25:Toxic by inhalation, in contact with skin and if swallowed .
R11:Highly Flammable.
[Safety Statements ]

S22:Do not breathe dust .
S24/25:Avoid contact with skin and eyes .
S45:In case of accident or if you feel unwell, seek medical advice immediately (show label where possible) .
S16:Keep away from sources of ignition-No smoking .
S7:Keep container tightly closed .
S36/37:Wear suitable protective clothing and gloves .
[RIDADR ]

3077
[WGK Germany ]

3
[RTECS ]

DB9440000
[HS Code ]

29039990
[Safety Profile]

Moderately toxic by ingestion. An experimental teratogen. Experimental reproductive effects. Irritant. Combustible liquid. When heated to decomposition it emits toxic fumes of Cl-. See also CHLORINATED HYDROCARBONS, AROMATIC.
[Hazardous Substances Data]

634-66-2(Hazardous Substances Data)
[Toxicity]

Acute oral LD50 for rats 1,167 mg/kg (quoted, RTECS, 1985).
Hazard InformationBack Directory
[General Description]

White to off-white crystals.
[Reactivity Profile]

Simple aromatic halogenated organic compounds, such as 1,2,3,4-TETRACHLOROBENZENE(634-66-2), are very unreactive. Reactivity generally decreases with increased degree of substitution of halogen for hydrogen atoms. Materials in this group may be incompatible with strong oxidizing and reducing agents. Also, they may be incompatible with many amines, nitrides, azo/diazo compounds, alkali metals, and epoxides.
[Air & Water Reactions]

Insoluble in water.
[Health Hazard]

ACUTE/CHRONIC HAZARDS: This compound may cause irritation of the skin.
[Fire Hazard]

This chemical is probably combustible.
[Chemical Properties]

WHITE CRYSTALLINE SOLID
[Definition]

ChEBI: A tetrachlorobenzene carrying chloro groups at positions 1, 2 , 3 and 4.
[Environmental Fate]

Biological. A mixed culture of soil bacteria or a Pseudomonas sp. transformed 1,2,3,4- tetrachlorobenzene to 2,3,4,5-tetrachlorophenol (Ballschiter and Scholz, 1980). After incubation in sewage sludge for 32 d under anaerobic conditions, 1,2,3,4-tetrachlorobenzene did not biodegrade (Kirk et al., 1989). The half-life of 1,2,3,4-tetrachlorobenzene in an anaerobic enrichment culture was 26.4 h (Beurskens et al., 1993). Potrawfke et al. (1998) reported that a pure culture of Pseudomonas chlororaphis RW71 mineralized 1,2,3,4-tetrachlorobenzene as a sole source of carbon and energy. Intermediate biodegradation products identified were tetrachlorocatechol, tetrachloromuconic acid, 2,3,5-trichlorodienelactone, 2,3,5-trichloro-4-hydroxymuconic acid. In an enrichment culture derived from a contaminated site in Bayou d’Inde, LA, 1,2,4,5- tetrachlorobenzene underwent reductive dechlorination yielding 1,2,4-trichlorobenzene. The maximum dechlorination rate, based on the recommended Michaelis-Menten model, was 208 nM/d (Pavlostathis and Prytula, 2000).
Photolytic. Irradiation (λ ≥285 nm) of 1,2,3,4-tetrachlorobenzene (1.1–1.2 mM/L) in an acetonitrile-water mixture containing acetone (0.553 mM/L) as a sensitizer gave the following products (% yield): 1,2,3-trichlorobenzene (9.2), 1,2,4-trichlorobenzene (32.6), 1,3-dichlorobenzene (5.2), 1,4-dichlorobenzene (1.5), 2,2′,3,3′,4,4′,5-heptachlorobiphenyl (2.52), 2,2′,3,3′,4,5,6′- heptachlorobiphenyl (1.22), 10 hexachlorobiphenyls (3.50), five pentachlorobiphenyls (0.87), dichlorophenyl cyanide, two trichloroacetophenones, trichlorocyanophenol, (trichlorophenyl) acetonitriles, and 1-(trichlorophenyl)-2-propanone (Choudhry and Hutzinger, 1984). Without acetone, the identified photolysis products (% yield) included 1,2,3-trichlorobenzene (7.8), 1,2,4- trichlorobenzene (26.8), 1,2-dichlorobenzene (0.5), 1,3-dichlorobenzene (0.7), 1,4-dichloro-benzene (30.4), 1,2,3,5-tetrachlorobenzene (2.26), 1,2,4,5-tetrachlorobenzene (0.72), 2,2′,3,3′,4,4′,5- heptachlorobiphenyl (<0.01), and 2,2′,3,3′,4,5,6′-heptachlorobiphenyl (<0.01) (Choudhry and Hutzinger, 1984). The sunlight irradiation of 1,2,3,4-tetrachlorobenzene (20 g) in a 100-mL borosilicate glass-stoppered Erlenmeyer flask for 56 d yielded 4,280 ppm heptachlorobiphenyl (Uyeta et al., 1976).
[Solubility in water]

Soluble in acetic acid, ether, ligroin (Weast, 1986), and very soluble in many chlorinated solvents including chloroform, carbon tetrachloride, etc.
[Purification Methods]

Crystallise it from EtOH. [Beilstein 5 H 204, 5 II 156, 5 III 550, 5 IV 667.]
Material Safety Data Sheet(MSDS)Back Directory
[msds information]

1,2,3,4-tetrachlorobenzene(634-66-2).msds
Spectrum DetailBack Directory
[Spectrum Detail]

1,2,3,4-Tetrachlorobenzene(634-66-2)MS
1,2,3,4-Tetrachlorobenzene(634-66-2)1HNMR
1,2,3,4-Tetrachlorobenzene(634-66-2)13CNMR
1,2,3,4-Tetrachlorobenzene(634-66-2)IR1
1,2,3,4-Tetrachlorobenzene(634-66-2)IR2
1,2,3,4-Tetrachlorobenzene(634-66-2)IR3
1,2,3,4-Tetrachlorobenzene(634-66-2)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

1,2,3,4-Tetrachlorobenzene, 98%(634-66-2)
[Sigma Aldrich]

634-66-2(sigmaaldrich)
[TCI AMERICA]

1,2,3,4-Tetrachlorobenzene,>96.0%(GC)(634-66-2)
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