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ChemicalBook--->CAS DataBase List--->42036-65-7

42036-65-7

42036-65-7 Structure

42036-65-7 Structure
IdentificationMore
[Name]

2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride
[CAS]

42036-65-7
[Synonyms]

2-(DIMETHYLAMINOMETHYL)-1-CYCLOHEXANONE HYDROCHLORIDE
2-(DIMETHYLAMINOMETHYL)-CYCLOHEXAN-1-ONE HCL
2-(DIMETHYLAMINOMETHYL) CYCLOHEXANONE HCL
2-[(DIMETHYLAMINO)METHYL]CYCLOHEXANONE HYDROCHLORIDE
2-(N,N-DIMETHYLAMINOMETHYL)CYCLOHEXANONE HCL
2-(Dimethylamino)methyl cyclhexanone hydrochloride
2-(Dimethylaminomethyl)-1-cyclohexanoneHCl
2-(Dimethylaminomethyl)-1-cyclohexanone, hydrochloride salt
2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride 98%
[Molecular Formula]

C9H18ClNO
[MDL Number]

MFCD00102580
[Molecular Weight]

191.7
[MOL File]

42036-65-7.mol
Chemical PropertiesBack Directory
[Appearance]

white crystalline powder
[Melting point ]

147-151 °C
[storage temp. ]

2-8°C
[solubility ]

Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
[form ]

Crystalline Powder
[color ]

White
[Water Solubility ]

soluble
[InChI]

InChI=1S/C9H17NO.ClH/c1-10(2)7-8-5-3-4-6-9(8)11;/h8H,3-7H2,1-2H3;1H
[InChIKey]

CLVHTSWMNNSUSH-UHFFFAOYSA-N
[SMILES]

C1(CN(C)C)CCCCC1=O.Cl
[CAS DataBase Reference]

42036-65-7(CAS DataBase Reference)
Safety DataBack Directory
[Safety Statements ]

S24/25:Avoid contact with skin and eyes .
[HS Code ]

29223900
Hazard InformationBack Directory
[Chemical Properties]

white crystalline powder
[Uses]

An impurity found in Tramadol (T712500).
[Synthesis]

0.982 g (1.03 mL, 10.0 mmol) cyclohexanone, 0.360 g (12.0 mmol) paraformaldehyde, 0.816 g (10.0 mmol) dimethylammonium chloride and 4 mL ethanol are filled in a 25 mL round bottom flask with reflux condenser and magnetic stir bar. 2 drops of conc. hydrochloric acid is added, and the mixture is heated under stirring for 4 hours under reflux. The hot solution is filtered in a round bottom flask, and the solvent is evaporated by the rotary evaporator. The residue is dissolved in 2 mL ethanol under heating. At room temperature, 20 mL acetone is added to the solution. For complete crystallization, the solution is stored overnight in the freezer compartment. The crystallized crude product 2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride is sucked off over a Buechner funnel and dried in the desiccator over silica gel.
2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

2-(Dimethylaminomethyl)-1-cyclohexanone hydrochloride, 98%(42036-65-7)
[Sigma Aldrich]

42036-65-7(sigmaaldrich)
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