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ChemicalBook--->CAS DataBase List--->2444-68-0

2444-68-0

2444-68-0 Structure

2444-68-0 Structure
IdentificationMore
[Name]

9-VINYLANTHRACENE
[CAS]

2444-68-0
[Synonyms]

9-VINYLANTHRACENE
9-Ethenyl anthracene
9-Vinylanthracene,97%
Anthracene, 9-ethenyl-
[EINECS(EC#)]

219-486-2
[Molecular Formula]

C16H12
[MDL Number]

MFCD00003576
[Molecular Weight]

204.27
[MOL File]

2444-68-0.mol
Chemical PropertiesBack Directory
[Appearance]

yellow to green crystalline solid
[Melting point ]

62-65 °C (lit.)
[Boiling point ]

61-66 °C/10 mmHg (lit.)
[density ]

1.1570 (estimate)
[refractive index ]

1.5000 (estimate)
[Fp ]

61-66°C/10mm
[storage temp. ]

2-8°C
[Detection Methods]

HPLC,NMR,MS
[BRN ]

2041641
[CAS DataBase Reference]

2444-68-0(CAS DataBase Reference)
Safety DataBack Directory
[Safety Statements ]

S22:Do not breathe dust .
S24/25:Avoid contact with skin and eyes .
[WGK Germany ]

3
[HS Code ]

29012990
Raw materials And Preparation ProductsBack Directory
[Raw materials]

Ethanol-->Methanol-->Tetrahydrofuran-->Acetic acid-->N,N-Dimethylformamide-->Phosphorus oxychloride-->Aluminum chloride-->Sodium borohydride-->Iodomethane-->p-Toluenesulfonic acid-->Acetyl chloride-->Sodium acetate-->Sodium azide-->Triphenylphosphine-->Tosyl chloride-->Oxalyl chloride-->Potassium tert-butoxide-->1,2-Dichloroethane-->Anisole-->1,2-Dichlorobenzene-->Methyl bromide-->Potassium bisulfate-->Anthracene-->DBU-->2-Pyrrolidinone-->Anthrone-->3-Chloro-1-propanol-->Vinylmagnesium bromide-->9-Anthraldehyde
[Preparation Products]

polyvinyl anthracene
Hazard InformationBack Directory
[Chemical Properties]

yellow to green crystalline solid
[Uses]

9-Vinylanthracene (cas# 2444-68-0) is a compound useful in organic synthesis.
[Synthesis Reference(s)]

The Journal of Organic Chemistry, 56, p. 4035, 1991 DOI: 10.1021/jo00012a043
Synthesis, p. 319, 1981
[Purification Methods]

Purify it by vacuum sublimation. It has also been purified by chromatography on silica gel with cyclohexane as eluent, and recrystallised from EtOH [Werst et al. J Am Chem Soc 109 32 1987]. [Beilstein 5 IV 2415.]
Spectrum DetailBack Directory
[Spectrum Detail]

9-VINYLANTHRACENE(2444-68-0)MS
9-VINYLANTHRACENE(2444-68-0)1HNMR
9-VINYLANTHRACENE(2444-68-0)13CNMR
9-VINYLANTHRACENE(2444-68-0)IR1
9-VINYLANTHRACENE(2444-68-0)IR2
9-VINYLANTHRACENE(2444-68-0)Raman
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

9-Vinylanthracene(2444-68-0)
[Alfa Aesar]

9-Vinylanthracene, 97%(2444-68-0)
[Sigma Aldrich]

2444-68-0(sigmaaldrich)
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