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ChemicalBook--->CAS DataBase List--->18546-37-7

18546-37-7

18546-37-7 Structure

18546-37-7 Structure
IdentificationMore
[Name]

2-Deoxy-L-ribose
[CAS]

18546-37-7
[Synonyms]

2-DEOXY-L-ERYTHRO-PENTOFURANOSE
2-DEOXY-L-RIBOSE
L-ERYTHRO-PENTOFURANOSE
2-DEOXY-L-RIBOSE 99%
L-erythro-Pentose, 2-deoxy-
[EINECS(EC#)]

606-054-7
[Molecular Formula]

C5H10O4
[MDL Number]

MFCD00132941
[Molecular Weight]

134.13
[MOL File]

18546-37-7.mol
Chemical PropertiesBack Directory
[Appearance]

white to light beige crystalline powder
[Melting point ]

69-72°C
[alpha ]

57 º (c=0.9 H2O after 24h)
[Boiling point ]

167.23°C (rough estimate)
[density ]

1.0590 (rough estimate)
[refractive index ]

1.4050 (estimate)
[storage temp. ]

2-8°C
[solubility ]

Methanol (Slightly), Water (Slightly)
[form ]

Solid
[pka]

13.58±0.20(Predicted)
[color ]

Light Yellow to Pale Beige
[optical activity]

[α]/D 54.0±2.0°, 24 hr, c = 1 in H2O
[CAS DataBase Reference]

18546-37-7(CAS DataBase Reference)
Safety DataBack Directory
[Hazard Codes ]

Xn,Xi
[Risk Statements ]

R20/21/22:Harmful by inhalation, in contact with skin and if swallowed .
R36/37/38:Irritating to eyes, respiratory system and skin .
[Safety Statements ]

S24/25:Avoid contact with skin and eyes .
S37/39:Wear suitable gloves and eye/face protection .
S36:Wear suitable protective clothing .
S26:In case of contact with eyes, rinse immediately with plenty of water and seek medical advice .
[HS Code ]

29329990
Hazard InformationBack Directory
[Chemical Properties]

white to light beige crystalline powder
[Uses]

2-Deoxy-L-ribose is an isomer of 2-Deoxy-D-ribose (D252000) which induces apoptosis by inhibiting the synthesis and increasing the efflux of glutathione.
[Definition]

ChEBI: 2-deoxy-L-arabinose is a deoxypentose. It is functionally related to a L-arabinose.
[Production Methods]

The provides the synthetic process of 2-Deoxy-L-ribose comprising the steps of; (A) protection step in which aldehyde group of 2-deoxy-D-ribose is protected in the form of acetal. 2-deoxy-l-O-alkyl-D-ribopyranoside is prepared by the reaction of 2-deoxy-D-ribose with alcohol in the presence of acid; (B) activation step in which 3 -and 4-OH groups of 2-deoxy-D-ribose are activated. 2-deoxy-l-O-alkyl- 3,4-di-(alkanesulfonyl)-D-ribose or 2-deoxy-1-O-alkyl-3,4-di-(arylsulfonyl)-D-ribose is prepared by reaction of the above 2-deoxy-l-O-alkyl-D-ribose with organic sulfonylhalide for activation of 3- and 4-OH; (C) inversion step in which stereochemistry of 3- and 4-OH groups is changed. Reaction of the above 2-deoxy-l- O-alkyl-3,4-di-(alkanesulfonyl)-D-ribose or 2-deoxy-l-O-alkyl-3,4-di-(arylsulfonyl)- D-ribose with a metal salt of organic acid leads to 2-deoxy-L-ribose derivatives of which stereochemistry of 3- and 4-OH is different from the corresponding 2-deoxy-D- ribose derivatives; (D) deprotection step in which 2-deoxy-L-ribose is prepared by consecutive reactions of the step (C) products with acid and base.
[Purification Methods]

Crystallise 2-deoxy--L-ribose from diethyl ether. It can also be purified by dissolving the ribose (7.3g) in EtOAc (3L) by reflux, decanting from any insoluble mate
Well-known Reagent Company Product InformationBack Directory
[Acros Organics]

2-Deoxy-L-ribose, 99%(18546-37-7)
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