| Identification | More | [Name]
4-(BROMOMETHYL)-BENZOIC ACID, 1,1-DIMETHYLETHYL ESTER | [CAS]
108052-76-2 | [Synonyms]
4-(BROMOMETHYL)-BENZOIC ACID, 1,1-DIMETHYLETHYL ESTER
4-BROMO METHYL BENZOIC ACID MONO TERT-BUTYL ESTER
TERT-BUTYL P-(BROMOMETHYL) BENZOATE
4-Bromomethyl-benzoic acid tert-butyl ester
t-butyl-4-bromomethylbenzoate
1,1-DIMETHYLETHYL 4-(BROMOMETHYL)BENZOATE | [EINECS(EC#)]
691-573-1 | [Molecular Formula]
C12H15BrO2 | [MDL Number]
MFCD04973450 | [Molecular Weight]
271.15 | [MOL File]
108052-76-2.mol |
| Chemical Properties | Back Directory | [Melting point ]
53-55 °C | [Boiling point ]
320.9±25.0 °C(Predicted) | [density ]
1.313±0.06 g/cm3(Predicted) | [storage temp. ]
Inert atmosphere,2-8°C | [solubility ]
DMF: 30 mg/ml; DMSO: 30 mg/ml; Ethanol: 30 mg/ml; Ethanol:PBS (pH 7.2)(1:3): .25 mg/ml | [form ]
A crystalline solid | [CAS DataBase Reference]
108052-76-2(CAS DataBase Reference) |
| Hazard Information | Back Directory | [Synthesis]
To a solution of substituted toluene in carbon tetrachloride were added N-bromosuccinimide (1.1 equiv) and 2,2'-azobis(isobutyronitrile) (0.15 equiv). The mixture was refluxed, then filtered and concentrated. The residue was purified by silica gel column chromatography to give tert-Butyl 4-(bromomethyl)benzoate.
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