Zeranol synthesis
- Product Name:Zeranol
- CAS Number:26538-44-3
- Molecular formula:C18H26O5
- Molecular Weight:322.4
36455-72-8
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26538-44-3
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Yield:26538-44-3 79%
Reaction Conditions:
with 5 mol% Pd/C;hydrogen in ethanol at 20;
Steps:
2.6General Procedure for Hydrogenation
General procedure: To a solution of zearalenonederivative (1.0 equiv) in EtOH (0.012 M) was added Pd/C (5 wt.%, 4 or 5 mol%).The mixture was stirred at room temperature under H2 atmosphere.After completion of the reaction, it was filtered through a pad of Celite,washed with EtOAc and concentrated in vacuo. Purification of the cruderesidue by column chromatography gave the pure hydrogenated compound.
References:
Tadpetch, Kwanruthai;Kaewmee, Benyapa;Chantakaew, Kittisak;Kantee, Kawalee;Rukachaisirikul, Vatcharin;Phongpaichit, Souwalak [Bioorganic and Medicinal Chemistry Letters,2016,vol. 26,# 15,p. 3612 - 3616] Location in patent:supporting information
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26538-44-3
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26538-44-3
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42422-68-4
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26538-44-3
99 suppliers
$89.79/1mg