virantmycin synthesis

4synthesis methods

Product Name:virantmycin
CAS Number:76417-04-4
Molecular formula:C19H26ClNO3
Molecular Weight:351.87

1H-Indole-1-carboxylic acid, 2,3-dihydro-5-iodo-2-(2-methoxyacetyl)-, 1,1-dimethylethyl ester, (2S)-

586390-84-3
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Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: Mg / tetrahydrofuran / -78 °C
1.2: 77 percent / tetrahydrofuran / 1 h / -78 °C
2.1: 59 percent / formic acid / CH₂Cl₂ / 2 h / 20 °C
3.1: 45 percent / tri-n-butylphosphine; carbon tetrachloride / CH₂Cl₂ / 1 h / Heating
4.1: 80 percent Turnov_. / K₂CO₃ / Pd(OAc)2 / H₂O; methanol / 18 h / 20 °C / 760 Torr

References:

Ori, Mayuko;Toda, Narihiro;Takami, Kazuko;Tago, Keiko;Kogen, Hiroshi [Tetrahedron,2005,vol. 61,# 8,p. 2075 - 2104]

79815-20-6 Synthesis

79815-20-6
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References

1H-Indole-2-carboxylicacid,2,3-dihydro-,methylester,(2S)-(9CI)

141410-06-2
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References

1H-Indole-1,2-dicarboxylic acid, 2,3-dihydro-, 1-(1,1-diMethylethyl) 2-Methyl ester, (2S)-

197460-36-9
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References

virantmycin Related Search:

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