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ChemicalBook CAS DataBase List Thionyl bromide
507-16-4

Thionyl bromide synthesis

7synthesis methods
Reaction of SO2 with Br2 in the presence of PCl3: 64 g. of SO2 is added to a mixture of 138 g. of PCl3 and 160 g. of Br2 , while the reactor is cooled. The yield, after fractional distillation, is 180 g. of SOBr2.
-

Yield:-

Reaction Conditions:

with phosphorus(V) oxybromide2 d in bomb tube;

References:

Behne, W.;Jander, G.;Hecht. H. [Zeitschrift fur Anorganische und Allgemeine Chemie][Zeitschrift fuer Anorganische und Allgemeine Chemie,1952,vol. 269,p. 249 - 261] [Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: S: SVol.3, 2.1.8.9.11, page 206 - 207]

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