Tetrahydrothiopyran-4-one synthesis
- Product Name:Tetrahydrothiopyran-4-one
- CAS Number:1072-72-6
- Molecular formula:C5H8OS
- Molecular Weight:116.18
111-17-1
283 suppliers
$6.00/25g
1072-72-6
279 suppliers
$10.00/1g
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 93 percent / TsOH / toluene / Heating
2: 1.) NaH, allyl alcohol / 1.) Et2O, room temp., 15 min; 2.) reflux, 4 h
3: 76 percent / morpholine / Pd(PPh3)4 / tetrahydrofuran / Ambient temperature
References:
Casy, Guy;Sutherland, Alan G.;Taylor, Richard J. K.;Urben, Peter G. [Synthesis,1989,# 10,p. 767 - 769]
17396-36-0
28 suppliers
$65.00/50mg
1072-72-6
279 suppliers
$10.00/1g
4160-61-6
87 suppliers
$36.00/250mg
1072-72-6
279 suppliers
$10.00/1g
4131-74-2
148 suppliers
$6.00/25g
1072-72-6
279 suppliers
$10.00/1g
26822-37-7
35 suppliers
$57.00/1g
1072-72-6
279 suppliers
$10.00/1g