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ChemicalBook CAS DataBase List TERT-OCTYL ISOTHIOCYANATE
17701-76-7

TERT-OCTYL ISOTHIOCYANATE synthesis

6synthesis methods
-

Yield:-

Reaction Conditions:

in sulfuric acid

Steps:

2 Preparation of 1-(dodecylbenzenesulfonyl)-4-t-octylthio-semicarbazide
The t-octylisothiocyanate was prepared from the reaction of diisobutylene and sodium thiocyanate as follows: A vigorously stirred mixture of diisobutylene and sodium thiocyanate was cooled in an ice bath and the sulfuric acid was added dropwise keeping the temperature between 30°-40°.

References:

Henkel Corporation US4237062, 1980, A

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