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ChemicalBook CAS DataBase List TERT-BUTYL 4-BROMOPYRIDIN-2-YLCARBAMATE
207799-10-8

TERT-BUTYL 4-BROMOPYRIDIN-2-YLCARBAMATE synthesis

7synthesis methods
30766-03-1 Synthesis
4-Bromopyridine-2-carboxylic acid

30766-03-1
267 suppliers
$7.00/1g

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Yield:207799-10-8 93%

Steps:


tert-Butyl (4-bromo-pyridin-2-yl)-carbamate (155)O HN^OT ohis c.omBrpound is prepared from 4-bromopyridine-2-carboxylic acid (154, 600 mg, 2.97 mmol) in accordance with the procedure of Deady, Korytsky and Rowe (Deady, L. W.; Korytsky, O. L.; Rowe, J. E. Aust. J. Chem., 1982, 35, 2025-2034). Yield: 750 mg (93%).

References:

CURIS, INC. WO2008/57497, 2008, A2 Location in patent:Page/Page column 293

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