tert-butyl 2,5-dihydrofuran-3-carboxylate synthesis

2synthesis methods

Product Name:tert-butyl 2,5-dihydrofuran-3-carboxylate
CAS Number:797038-34-7
Molecular formula:C9H14O3
Molecular Weight:170.21

797038-32-5 Synthesis

4-Oxo-Tetrahydro-Furan-3-Carboxylic Acid Tert-Butyl Ester

797038-32-5
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tert-butyl 2,5-dihydrofuran-3-carboxylate

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 89 percent / NaBH₄ / propan-2-ol / 0 - 20 °C
2: 91 percent / PPh₃; DIAD / tetrahydrofuran / 20 °C

References:

Bunnage, Mark E.;Davies, Stephen G.;Roberts, Paul M.;Smith, Andrew D.;Withey, Jonathan M. [Organic and Biomolecular Chemistry,2004,vol. 2,# 19,p. 2763 - 2776]

tert-butyl 4-hydroxytetrahydrofuran-3-carboxylate

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References

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