sodium dodecane-1-thiolate synthesis
- Product Name:sodium dodecane-1-thiolate
- CAS Number:26960-77-0
- Molecular formula:C12H27NaS
- Molecular Weight:226.4
Yield:-
Reaction Conditions:
in methanol at 20; for 0.25 h;
Steps:
2.2; 3.2
2) Preparation of Sodium Dodecanethiolate In another flask, sodium methoxide (1.43 g, 26 mmol) was dissolved in 10 ml methanol, and dodecanethiol (6.5 ml, 27 mmol) was added. The resulting solution was stirred at room temperature for 15 minutes. The solvent was then evaporated under reduced pressure at 90° C. 2) Preparation of Sodium Dodecanethiolate In another flask, sodium methoxide (8.1 g, 150 mmol) was dissolved in 10 ml methanol, and dodecanethiol (32.8 ml, 136.6 mmol) was added. The resulting solution was stirred at room temperature for 15 minutes. The solvent was then evaporated under reduced pressure at 90° C. Traces of methanol were evaporated by adding toluene and evaporating it at reduced pressure at 100° C. for two hours.
References:
US2008/139849,2008,A1 Location in patent:Page/Page column 5
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