SB 202190 synthesis
- Product Name:SB 202190
- CAS Number:152121-30-7
- Molecular formula:C20H14FN3O
- Molecular Weight:331.34
403-43-0
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$9.00/25g
152121-30-7
199 suppliers
$14.00/5mg
Yield:-
Steps:
Multi-step reaction with 5 steps
1: 100 percent / Et3N / CH2Cl2 / 0.5 h
2: 1.) LDA / 1.) THF, hexane, -78 deg C, 15 min, 2.) THF, hexane, from -78 deg C to RT
3: 74 percent / 3 N aq. HCl, NaNO2 / 0.5 h / Ambient temperature
4: NH4OAc, CH3CO2H / 18 h / Heating
5: P(OEt)3 / dimethylformamide / 2 h / 100 °C
References:
Gallagher, Timothy F.;Seibel, George L.;Kassis, Shouki;Laydon, Jeffrey T.;Blumenthal, Mary Jane;Lee, John C.;Lee, Dennis;Boehm, Jeffrey C.;Fier-Thompson, Susan M.;Abt, Jeffrey W.;Soreson, Margaret E.;Smietana, Juanita M.;Hall, Ralph F.;Garigipati, Ravi S.;Bender, Paul E.;Erhard, Karl F.;Krog, Arnold J.;Hofmann, Glenn A.;Sheldrake, Peter L.;McDonnell, Peter C.;Kumar, Sanjay;Young, Peter R.;Adams, Jerry L. [Bioorganic and Medicinal Chemistry,1997,vol. 5,# 1,p. 49 - 64]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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152121-30-7
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$14.00/5mg
116332-54-8
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$6.00/1g
152121-30-7
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$14.00/5mg
117423-41-3
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$75.00/100 mg
152121-30-7
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$14.00/5mg
108-89-4
328 suppliers
$15.00/25mL
152121-30-7
199 suppliers
$14.00/5mg