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ChemicalBook CAS DataBase List S-(4-NITROBENZYL)-6-THIOINOSINE
38048-32-7

S-(4-NITROBENZYL)-6-THIOINOSINE synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: 94 percent / hexamethyldisilazane; Me3SiCl; trimethylsilyl triflate / acetonitrile / 2.5 h / Heating
2.1: 36 percent / NH3 / methanol / 20 °C
3.1: trityl resin; pyridine / 48 h
3.2: Et3N / methanol / 5 h / 55 °C
3.3: 94 percent / triisopropylsilane; trifluoroacetic acid / CH2Cl2 / 0.17 h

References:

Yadav, Vikas;Chu, Chung K.;Rais, Reem H.;Al Safarjalani, Omar N.;Guarcello, Vincenzo;Naguib, Fardos N. M.;El Kouni, Mahmoud H. [Journal of Medicinal Chemistry,2004,vol. 47,# 8,p. 1987 - 1996]