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ChemicalBook CAS DataBase List Propyl propionate
106-36-5

Propyl propionate synthesis

15synthesis methods
Propyl propionate was synthesized by esterification of propyl alcohol with the corresponding acid in the presence of concentrated H2SO4, or in the presence of BF3.
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Yield:106-36-5 99%

Reaction Conditions:

with [{(PhN)MeC(Nt-Bu)}AlMe(μ-OMe)]2 at 20; for 0.5 h;Inert atmosphere;Schlenk technique;Green chemistry;Tishchenko-Claisen Dismutation;

Steps:

2.5 General procedure employed for the Tishchenko reaction

General procedure: The pre-catalyst, amidinatoaluminum compound (0.8 mmol) was placed in a dry Schlenk flask under a nitrogen atmosphere, and freshly distilled aldehyde (80 mmol) was introduced. The mixture was immediately stirred at room temperature for 30 min to produce the corresponding ester. The reaction was quenched with 0.5 ml of water and the product was distilled to collect the corresponding ester. The yields reported are the isolated yield.

References:

Zhang, Shaofeng;Han, Hongfei;Guo, Zhiqiang;Tong, Hongbo;Wei, Xuehong [Polyhedron,2015,vol. 90,p. 118 - 122]

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