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870-30-4

PHOSPHOROISOCYANATIDIC DICHLORIDE synthesis

12synthesis methods
-

Yield:870-30-4 90%

Reaction Conditions:

in neat (no solvent);heating very slow (due to danger of explosion) to 80°C with formation of liquid residue;; distillation;;

References:

Kirsanov, A. V. [1954,vol. 24,p. 1033 - 1038][C. A.,1955,p. 8787] [Gmelin Handbuch der Anorganischen Chemie,Gmelin Handbook: P: MVol.C, 274, page 629 - 631]