NSC26054 synthesis
- Product Name:NSC26054
- CAS Number:7148-01-8
- Molecular formula:C11H11ClO3
- Molecular Weight:226.658
Yield:7148-01-8 99%
Reaction Conditions:
with N-Bromosuccinimide at 70; for 20 h;
Steps:
3.2.1. General Procedure for the Esterification between Carboxylic Acids and Alcohols
General procedure: The mixture of carboxylic acid, alcohol and N-bromosuccinimide was stirred in a 25 mL reactortube at 70 °C for 2-40 h. After the completion of the reaction, the mixture was cooled to roomtemperature and alcohol was evaporated under reduced pressure. The isolation procedure was as follows, except where noted differently in Section 3.2.6. The residue was dissolved in ethyl acetate andconsecutively washed with 10 mL of 10% Na2S2O3 (aq), 5 mL of saturated NaHCO3 (aq) and 10 mL ofdistilled water. The water phase was extracted with ethyl acetate (3Χ5 mL). The organic layers were combined, dried over Na2SO4 and the solvent was evaporated under reduced pressure.
References:
?ebular, Klara;Bo?i?, Bojan ?.;Stavber, Stojan [Molecules,2018,vol. 23,# 9,art. no. 2235]
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