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ChemicalBook CAS DataBase List Nitrogen Tetroxide
10544-72-6

Nitrogen Tetroxide synthesis

10synthesis methods
Nitrogen tetroxide always is formed along with nitrogen dioxide during preparation of the dioxide (See Nitrogen Dioxide.) Mixed oxides are produced by oxidation of nitric oxide (NO) in air, heating metal nitrates, or by metals reacting with nitric acids or nitrates.
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Yield:-

Reaction Conditions:

with nitrosylsulfuric acid;sulfuric acidInert atmosphere;

Steps:


In a 100 mL Teflon threenecked-flask, multicrystalline silicon wafer pieces were added to freshly prepared etching mixture (25 mL). To avoid oxidation of nitrogen oxides and hydrolysis of trifluorosilane, all etching experiments were performed under argon. Depending on the reactivity of the etching mixture, the reaction time for each experiment varied from 120 to 600 s.

References:

Lippold, Marcus;Boehme, Uwe;Gondek, Christoph;Kronstein, Martin;Patzig-Klein, Sebastian;Weser, Martin;Kroke, Edwin [European Journal of Inorganic Chemistry,2012,# 34,p. 5714 - 5721]

10102-44-0 Synthesis
NITROGEN DIOXIDE

10102-44-0
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Nitrogen Tetroxide

10544-72-6
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