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ChemicalBook CAS DataBase List N-TRICOSANE
638-67-5

N-TRICOSANE synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.25 h / -78 °C
1.2: -78 - 20 °C
2.1: n-butyllithium / tetrahydrofuran / -78 - 0 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: palladium 10% on activated carbon; hydrogen

References:

Vidal, Diogo M.;Fávaro, Carla F.;Guimar?es, Matheus M.;Zarbin, Paulo H. G. [Journal of the Brazilian Chemical Society,2016,vol. 27,# 8,p. 1506 - 1511]

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