N-FORMYL-1,2,3,4-TETRAHYDROISOQUINOLINE synthesis
14synthesis methods
- Product Name:N-FORMYL-1,2,3,4-TETRAHYDROISOQUINOLINE
- CAS Number:1699-52-1
- Molecular formula:C10H11NO
- Molecular Weight:161.2
Yield:1699-52-1 99%
Reaction Conditions:
with CF3O3S(1-)*C25H42N6Rh(1+);diphenylsilane in dichloromethane at 25; under 19001.3 Torr; for 4 h;High pressure;Autoclave;
References:
Nguyen, Thanh V. Q.;Yoo, Woo-Jin;Kobayashi [Angewandte Chemie - International Edition,2015,vol. 54,# 32,p. 9209 - 9212][Angew. Chem.,2015,vol. 127,# 32,p. 9341 - 9344,4] Location in patent:supporting information