N-(CYANOMETHYL)ACETAMIDE synthesis
- Product Name:N-(CYANOMETHYL)ACETAMIDE
- CAS Number:4814-80-6
- Molecular formula:C4H6N2O
- Molecular Weight:98.1
6011-14-9
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10387-40-3
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$10.00/1g
4814-80-6
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$58.00/100mg
Yield:4814-80-6 99 %Spectr.
Reaction Conditions:
with sodium hydroxide;potassium hexacyanoferrate(III) in water at 20; pH=9; for 0.333333 h;
Steps:
Acetylation of α-aminonitriles with thioacetate.
General procedure: α-Aminonitrile hydrochloride (AA-CN*HCl; 50 mM) and potassium thioacetate (AcSK; 150 mM) were dissolved in H2O (2 ml) and the solution was adjusted topH 9.0 with NaOH. Potassium hexacyanoferrate(III) (K3[Fe(CN)6]; 450 mM) was added, and the solution was stirred at room temperature for 20 min. The solution was adjusted to pH 9.0 and centrifuged, and NMR spectra of the supernatant were acquired. Yields are reported in Table 1 and characterization data in Supplementary Information.
References:
Canavelli, Pierre;Islam, Saidul;Powner, Matthew W. [Nature,2019,vol. 571,# 7766,p. 546 - 549]
6011-14-9
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$5.00/10g
108-24-7
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$14.00/250ML
4814-80-6
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$58.00/100mg
108-24-7
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151-63-3
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$50.00/25g
4814-80-6
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$58.00/100mg
75-36-5
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540-61-4
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4814-80-6
36 suppliers
$58.00/100mg
6011-14-9
379 suppliers
$5.00/10g
75-36-5
589 suppliers
$17.92/100G
4814-80-6
36 suppliers
$58.00/100mg