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ChemicalBook CAS DataBase List N-Boc-3-bromo-4-fluoroaniline
836619-77-3

N-Boc-3-bromo-4-fluoroaniline synthesis

3synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
833 suppliers
$13.50/25G

656-64-4 Synthesis
3-Bromo-4-fluoroaniline

656-64-4
257 suppliers
$8.00/5g

-

Yield:836619-77-3 100%

Reaction Conditions:

Stage #1: 3-bromo-4-fluoroanilinewith triethylamine in tetrahydrofuran;water at 20; for 0.0833333 h;
Stage #2: di-tert-butyl dicarbonate in tetrahydrofuran;water at 0 - 20; for 6 h;

References:

Awuah, Samuel G.;George, Nathaniel;Ofori, Samuel;Parkin, Sean [RSC Advances,2020,vol. 10,# 40,p. 24017 - 24026]

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