N-(2-CHLOROBENZYL)PROP-2-EN-1-AMINE synthesis
- Product Name:N-(2-CHLOROBENZYL)PROP-2-EN-1-AMINE
- CAS Number:103754-08-1
- Molecular formula:C10H12ClN
- Molecular Weight:181.66
57966-12-8
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103754-08-1
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Yield:103754-08-1 82%
Reaction Conditions:
Stage #1: o-Chlorbenzylidenallylaminwith C21H39NPPd(1-)*C2F3O2(1-);phenylsilane in chloroform-d1 at 40; for 16 h;Glovebox;Sealed tube;
Stage #2: with water in chloroform-d1;Sealed tube;Glovebox;regioselective reaction;
References:
Tafazolian, Hosein;Schmidt, Joseph A.R. [Catalysis science and technology,2016,vol. 6,# 3,p. 685 - 689]