METHYL1-BENZYL-PIPERIDINE-2-CARBOXYLATE synthesis
- Product Name:METHYL1-BENZYL-PIPERIDINE-2-CARBOXYLATE
- CAS Number:124619-69-8
- Molecular formula:C14H19NO2
- Molecular Weight:233.31
![Chromium, pentacarbonyl[1-(phenylmethyl)-2-piperidinylidene]-, (OC-6-21)-](/CAS/20211123/GIF/124685-64-9.gif)
Yield:124619-69-8 90%
Reaction Conditions:
with methanol in methanol;Irradiation (UV/VIS); solid carbene complex is added to an oven-dried Pyrex pressure tube, followed by dry methanol, contents are degassed, purged with Ar, warmed to room temp., purged with CO, pressurized with 50-90 psi CO, irradiated (450 W) for 6 d; monitored by TLC, mixt. is filtered (Celite), evapg. in vacuo yields pure product; NMR, IR, elem. anal.;
References:
Hegedus, Louis S.;Schwindt, Mark A.;De Lombaert, Stéphane;Imwinkelried, Rene [Journal of the American Chemical Society,1990,vol. 112,# 6,p. 2264 - 2273]
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