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ChemicalBook CAS DataBase List METHYL HEPTADECANOATE
1731-92-6

METHYL HEPTADECANOATE synthesis

3synthesis methods
-

Yield:-

Reaction Conditions:

with mesoporous HZSM-5 zeolite at 500;

Steps:

2.4. Catalytic performance tests
General procedure: Catalytic performance of catalysts was evaluated by catalytic cracking of ethanol and oleic acid in a fixed-bed quartz tube reactor(inner diameter: 20 mm; length: 380 mm). As a typical run, the catalyst(0.5 g) was loaded into reactor, and heated to a desired temperature inN2 stream (the flow rate: 40 mL/min). The feedstock (0.87 g) was then injected into the reactor by a syringe pump. After flowing out from the reactor, the reaction products were cooled. Liquid products were weighed and analyzed by GC-MS (QP5000, Shimadzu, Japan) equipped with a DB-WAX fused silica capillary column (30m×0.25mm×0.25 μm). The gaseous product was collected with a gas collecting bag,and analyzed by GC referring to the method as described in our previous study

References:

Zhao, Tingting;Li, Fuwei;Yu, Hongchang;Ding, Shilei;Li, Zhixia;Huang, Xinyuan;Li, Xiang;Wei, Xiaohan;Wang, Zhenlin;Lin, Hongfei [Applied Catalysis A: General,2019,vol. 575,p. 101 - 110]

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