METHYL-3-N-ACETYLAMINO PHTHALATE synthesis
- Product Name:METHYL-3-N-ACETYLAMINO PHTHALATE
- CAS Number:52659-18-4
- Molecular formula:C12H13NO5
- Molecular Weight:251.24
67-56-1
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Yield:52659-18-4 90%
Reaction Conditions:
with graphite phase carbon nitride supported cuprous catalyst (g-C3N4/Cu2O) at 20; for 12 h;
Steps:
3-4 Example 4
Weigh compound 1 (1mmol) and dissolve it in methanol (12mL),Add 300mg of product B and acetic anhydride (3.0mmol) at room temperature, stir and react for 12 hours,After filtering, the filtrate is concentrated under reduced pressure,After silica gel column chromatography (EtOAc/petroleum ether = 1/20 to 1/15), compound 2 (226 mg, 90.0%) was obtained.
References:
CN111499533,2020,A Location in patent:Paragraph 0021-0026
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