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ChemicalBook CAS DataBase List METHYL 2-NONYNOATE
111-80-8

METHYL 2-NONYNOATE synthesis

7synthesis methods
From 2-octene by way of 1-octyne and octyne carboxylic acid.
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 90 percent / tetrabutylammonium tetrafluoroborate; Mg anode; Ag cathode / dimethylformamide / 3 h / 20 °C / 380.03 Torr / Electrochemical reaction
2: K2CO3 / dimethylformamide / 12 h / 50 °C

References:

Ko?ster, Frank;Dinjus, Erkhardt;Din?ach, Elisabet [European Journal of Organic Chemistry,2001,# 13,p. 2507 - 2511]

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