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ChemicalBook CAS DataBase List METHYL 2,4-DIFLUOROBENZOATE
106614-28-2

METHYL 2,4-DIFLUOROBENZOATE synthesis

6synthesis methods
-

Yield:106614-28-2 100%

Reaction Conditions:

at 20; for 2 h;

Steps:

6.1

To 100 mL of MeOH, 2,4-difluorobenzoyl chloride (10 mL, 79.3 mmol) was added and the mixture stirred at room temperature for 2 hours. The solvent was then evaporated affording the tilte compound as pale yellow oil (quantitative).IH-NMR (400 MHz), δ (ppm, DMSOtZ6): 8.0 (m, IH), 7.44 (m, IH), 7.25 (m, IH),3.87 (s, 3H).

References:

WO2007/68619,2007,A1 Location in patent:Page/Page column 97

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