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ChemicalBook CAS DataBase List METHYL 2,2':6',2''-TERPYRIDINE-4'-CARBOXYLATE
247058-06-6

METHYL 2,2':6',2''-TERPYRIDINE-4'-CARBOXYLATE synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1.1: 100 percent / 15 percent NaOH / methanol / 2 h / 0 °C
2.1: 60 percent / Et2NH / methanol / 48 h / 20 °C
3.1: AcONH4 / ethanol / 5 h
4.1: 68 percent / KMnO4; pyridine / H2O / 24 h / 20 °C
5.1: POCl3; PCl5 / 1.5 h / Heating
5.2: 3 percent / 0.5 h / Heating

References:

Raboin;Kirsch;Beley [Journal of Heterocyclic Chemistry,2000,vol. 37,# 5,p. 1077 - 1080]

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