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ChemicalBook CAS DataBase List METHYL 15-HYDROXYPENTADECANOATE
76529-42-5

METHYL 15-HYDROXYPENTADECANOATE synthesis

12synthesis methods
-

Yield:76529-42-5 98%

Reaction Conditions:

for 3 h;Heating / reflux;

Steps:

1
Methanol (150 mL) was added with 15-pentadecalactone (25.6 g), further added with 28% sodium methoxide solution (50 mL) and refluxed for 3 hours. The reaction solution was added with 1 N hydrochloric acid and extracted three times with ethyl acetate. The organic layer was washed with saturated brine and dried over anhydrous magnesium sulfate, and the solvent was removed to obtain methyl 15-hydroxypentadecanoate (28.5 g, yield: 98%).

References:

Fuji Photo Film Co. Ltd. EP1426353, 2004, A1 Location in patent:Page 14

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