H-PRO-GLY-GLY-OH synthesis
- Product Name:H-PRO-GLY-GLY-OH
- CAS Number:7561-25-3
- Molecular formula:C9H15N3O4
- Molecular Weight:229.23
37700-65-5
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7561-25-3
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Yield:7561-25-3 85%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in methanol at 20; under 760.051 Torr; for 2 h;
Steps:
Deprotection of Cbz of Cbz-protected tipeptide
General procedure: To a solution of Cbz-protected tripeptide (2 mmol) in MeOH (30 mL), 10% Pd/C was added at room temperature. After stirred under hydrogen (1 atm) for 2 h at room temperature, The resulting mixture was filtered. After the removal of solvent under reduced pressure, corresponding tripeptide was obtained.
References:
Kon, Kazumasa;Kohari, Yoshihito;Murata, Miki [Tetrahedron Letters,2019,vol. 60,# 5,p. 415 - 418] Location in patent:supporting information
3304-59-4
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7561-25-3
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1148-11-4
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61058-42-2
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2766-18-9
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7561-25-3
49 suppliers
$46.36/100MG