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ChemicalBook CAS DataBase List H-GLU(ANILIDE)-OH
5963-60-0

H-GLU(ANILIDE)-OH synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 6 steps
1: 98 percent / triethylamine / methanol / 3 h
2: 90 percent / toluenesulfonic acid / toluene / 3 h / Heating
3: thionyl chloride / CH2Cl2 / 0.5 h / Heating
4: pyridine / CH2Cl2 / 0.25 h / 20 °C
5: lithium hydroxide / tetrahydrofuran; H2O / 0.5 h / 5 °C
6: hydrogen / Pd/C / methanol

References:

Esslinger, C. Sean;Cybulski, Kimberly A.;Rhoderick, Joseph F. [Bioorganic and Medicinal Chemistry,2005,vol. 13,# 4,p. 1111 - 1118]

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