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ChemicalBook CAS DataBase List DL-GLYCERALDEHYDE
56-82-6

DL-GLYCERALDEHYDE synthesis

14synthesis methods
-

Yield:56-82-6 91%

Reaction Conditions:

with oxygen in water at 45 - 50; for 5 h;Reagent/catalyst;

Steps:

5; 6 Example 5
After the addition of Product A (8mg) to the aqueous glycerol solution (0.4mol/L, 500mL) and heated to 45-50 °C, bubbling of oxygen (flow rate of 150mL/min), 5 hours, centrifuged to remove the product A, supernatant after the solution was distilled off under reduced pressure and water was added crystallization from absolute ethanol, filtered, washed and dried to obtain the glyceraldehyde (16.4 g, yield 91.0%), consistent with the known structural data confirmed reports.

References:

Yangzhou Industry Polytechnic College;Chen Kequan;Liu Wei;Luo Zhichen;Zuo Zhifang CN108752309, 2018, A Location in patent:Paragraph 0048-0053

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