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179114-94-4

dimethyl 2-isocyanatoterephthalate synthesis

2synthesis methods
32315-10-9 Synthesis
Triphosgene

32315-10-9
416 suppliers
$10.00/1g

5372-81-6 Synthesis
Dimethyl aminoterephthalate

5372-81-6
226 suppliers
$17.67/5gm:

-

Yield:179114-94-4 100%

Reaction Conditions:

with sodium hydrogencarbonate in dichloromethane;water at 0; for 1 h;Inert atmosphere;

References:

Wu, Jing;Zhang, Jinzhu;Soto-Acosta, Ruben;Mao, Lili;Lian, Jiahui;Chen, Kenny;Pillon, Guy;Zhang, Guoqi;Geraghty, Robert J.;Zheng, Shengping [Journal of Organic Chemistry,2020,vol. 85,# 6,p. 4515 - 4524]

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