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ChemicalBook CAS DataBase List Dibenzyl azodicarboxylate
2449-05-0

Dibenzyl azodicarboxylate synthesis

2synthesis methods
PIDA (phenyliodine diacetate) and DCM (dichloromethane) were added to compound dibenzyl hydrazine-1,2-dicarboxylate, and the mixture was reacted with stirring at room temperature for 30 minutes to obtain DBAD (dibenzyl azodicarboxylate) in a yield of 97%.Dibenzyl azodicarboxylate
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Yield:2449-05-0 97%

Reaction Conditions:

with [bis(acetoxy)iodo]benzene in dichloromethane at 20; for 0.5 h;

Steps:

1 [Experimental Example 1]

PIDA (phenyliodine diacetate) and DCM (dichloromethane) were added to Compound 5, and the mixture was reacted with stirring at room temperature for 30 minutes to obtain DBAD (dibenzyl azodicarboxylate) in a yield of 97%.

References:

KR2021/153284,2021,A Location in patent:Paragraph 0269-0270; 0273-0274

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