DIALLYLAMINE HYDROCHLORIDE synthesis
- Product Name:DIALLYLAMINE HYDROCHLORIDE
- CAS Number:6147-66-6
- Molecular formula:C6H12ClN
- Molecular Weight:133.62
124-02-7
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$14.00/5mL
6147-66-6
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$14.00/1g
Yield:-
Reaction Conditions:
with hydrogenchloride in water at 20;
Steps:
1.2 2. Preparation of diallylamine hydrochloride
Pump the diallylamine into the kettle and start stirring.Pass the jacket cooling water to lower the temperature of the kettle to below 20 °C, pump the hydrochloric acid into the high tank, and slowly add hydrochloric acid at normal pressure.The molar ratio of N-methyldiallylamine to hydrochloric acid is 1:1, and the mixture is kept for 1-2 hours after the dropwise addition, and the reaction is completed to obtain diallylamine hydrochloride.
References:
Zouping Mingxing Chemical Co., Ltd.;Chen Qiang;Zhang Peng;Xu Xiaobo;Wang Tao;Sun Fantong;Du Xiaoyang;Zhang Junling CN109369413, 2019, A Location in patent:Paragraph 0047; 0054; 0055