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ChemicalBook CAS DataBase List Dehydrocorydaline
30045-16-0

Dehydrocorydaline synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: copper(l) iodide; benzoic acid / toluene / 12 h / 80 °C / Inert atmosphere; Molecular sieve
2: potassium carbonate / methanol / 0.5 h / 20 °C / Inert atmosphere
3: sodium formate; tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide; water / 1 h / 100 °C / Inert atmosphere
4: rhodium(III) chloride trihydrate; oxygen / ethanol / 8 h / 80 °C

References:

Zhou, Shiqiang;Tong, Rongbiao [Chemistry - A European Journal,2016,vol. 22,# 21,p. 7084 - 7089]

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