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ChemicalBook CAS DataBase List Decyl methacrylate
3179-47-3

Decyl methacrylate synthesis

5synthesis methods
-

Yield: 100%

Reaction Conditions:

with sulfuric acid at 20; for 48 h;

Steps:

Synthesis of decyl methacrylate monomer (9)
Monomer 9 was synthesised following a previously publishedmethod (Yildiz et al., 2011). 250 mg of methacrylic acid 4(2.9 mmol), were added to 5 ml of 1-decanol 8 and sulfuric acidin catalytic amounts. The solution was stirred for 48 h at roomtemperature. After reaction the mixture was purified by silica gelchromatography eluting with Exane/EtOAc, gradient from 100%Exane to 95:5 to give compound 9 in quantitative yield.

References:

Martin, Chloe;Marino, Nino;Curran, Ciara;McHale, Anthony P.;Callan, John F.;Callan, Bridgeen [International Journal of Pharmaceutics,2016,vol. 511,# 1,p. 570 - 578]

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