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5422-01-5

α-Butylpiperonyl Alcohol synthesis

3synthesis methods
-

Yield:5422-01-5 94.2%

Reaction Conditions:

Stage #1: 1-bromo-butanewith magnesium in diethyl ether at 0 - 5;
Stage #2: piperonal in diethyl ether;

References:

Koul, Surrinder;Koul, Jawahir Lal;Singh, Budh;Kapoor, Munish;Parshad, Rajinder;Manhas, Kuldeep S.;Taneja, Subhash C.;Qazi, Ghulam N. [Tetrahedron Asymmetry,2005,vol. 16,# 15,p. 2575 - 2591]