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ChemicalBook CAS DataBase List BIS(TRIMETHYLSILYL)CHLOROMETHANE
5926-35-2

BIS(TRIMETHYLSILYL)CHLOROMETHANE synthesis

9synthesis methods
a convenient one-pot procedure has been developed by Kemp and Cowley in which trimethylsilylchloride reacts with dichloromethane in the presence of nBuLi at ?110°Cto give bis(trimethylsilyl)dichloromethane.1 This intermediate is sequentially treated with nBuLi and ethanol to yield chlorobis(trimethylsilyl)methane. A number of other syntheses have been described
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Yield:5926-35-2 3% ，15951-41-4 3% ，5926-38-5 94%

Reaction Conditions:

with N,N,N,N-tetraethylammonium tetrafluoroborate in N,N-dimethyl-formamide; for 29.25 h;electroreduction, anode: Zn, cathode: stainless steel;

References:

Pons, P.;Biran, C.;Bordeau, M.;Dunogues, J. [Journal of Organometallic Chemistry,1988,vol. 358,p. 31 - 38]

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