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ChemicalBook CAS DataBase List Bis(4-bromophenyl) ether
2050-47-7

Bis(4-bromophenyl) ether synthesis

10synthesis methods
-

Yield:2050-47-7 82%

Reaction Conditions:

with titania nanoparticles supported on silica for 0.333333 h;

Steps:

2 Example 2 Preparation of dibromo diphenylether-18
SiO2-TiO2 (0.05 g) and p-bromophenol (1.73 g) were mixed well in a mortar,Grinding for 20 minutes,The product was separated by column chromatography on silica gel using n-hexane as eluant to give 1.34 g of a white solid in 82% yield.

References:

Shandong Analysis Beta Center;Ji Wenhua;Zhao Rusong;Wang Xiao;Geng Yanling;Wang Xia CN106957218, 2017, A Location in patent:Paragraph 0048-0050

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