BETA-D-GAL-[1->4]-BETA-D-GLCNAC-1->O-CETE synthesis
- Product Name:BETA-D-GAL-[1->4]-BETA-D-GLCNAC-1->O-CETE
- CAS Number:87019-31-6
- Molecular formula:C20H35NO13S
- Molecular Weight:529.56
86651-39-0
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87019-31-6
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 81 percent / cesium carbonate / dimethylformamide / 2 h / Ambient temperature
2: 39 percent / 1.) sodium methoxyde; 2.) hydrazine hydrate; / 1.) methanol, overnight; 2.) ethanol, 3.5 h, reflux; 3.) ethanol-water, 3 h, r.t.
References:
Dahmen, Jan;Frejd, Torbjoern;Groenberg, Gunnar;Lave, Thomas;Magnusson, Groeran;Noori, Ghazi [Carbohydrate Research,1983,vol. 118,p. 292 - 301]