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ChemicalBook CAS DataBase List BETA,4-DINITROSTYRENE
3156-41-0

BETA,4-DINITROSTYRENE synthesis

11synthesis methods
-

Yield:3156-41-0 99%

Reaction Conditions:

with bridged diamino-functionalized periodic mesoporous organosilicas with high nitrogen contents at 90; for 5 h;Henry Nitro Aldol Condensation;

Steps:

Activity test

General procedure: The Reaction 2 was carried out at 90 °C by stirring a mixture containing a catalyst with 0.024 mmol nitrogen, 1.0 mmol aldehyde, 4.0 mL nitromethane and n-decane as an internal standard. After reaction for 5 h, product analysis was performed on the GC under the above identical conditions.

References:

Zhu, Feng-Xia;Zhao, Pu-Su;Sun, Xiao-Jun;An, Li-Tao;Deng, Yong;Wu, Jia-Min [Journal of Solid State Chemistry,2017,vol. 255,p. 70 - 75]

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