Berberine chloride hydrate synthesis
- Product Name:Berberine chloride hydrate
- CAS Number:68030-18-2
- Molecular formula:C20H20ClNO5
- Molecular Weight:389.83
68030-18-2
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Yield:15401-69-1 80%
Reaction Conditions:
at 190; under 20 - 30 Torr; for 2 h;Calcination;
Steps:
1 Example 1 Preparation of berberrubine chloride
Take 10g of berberine hydrochloride into a three-burning screen,The calcination reaction was heated at 190 ° C under a vacuum of 20-30 mmHg for 2 h.Get 7.2g brown red product,spare. The yield is 80%;
References:
CN108948000,2018,A Location in patent:Paragraph 0012; 0013